• 10.15227/orgsyn.041.0041
  • Organic Syntheses
  • p 41-41, Volume 41, Issue 41,
  • journal-article


Reliable Procedure

The procedure described in this paper is very reliable. The ozone should be used in a fully functional fume hood as described.

1. Synthesized 10.1 g of crude diphenaldehyde starting from 10.0 g of phenanthrene.

2. The crude 1H-NMR of product is 80% clean and was easily...