| /paper/doi/10.1021/jo01343a026 | 0.000000 | 0.000000 |
| INIT | 0.002116 | 0.002116 |
| _initView | 0.007624 | 0.009740 |
| _initViewBasic | 0.000872 | 0.010612 |
| _initSiteModules | 0.001719 | 0.012331 |
| _initRouters | 0.001550 | 0.013881 |
| pre dispatch _ | 0.012720 | 0.026601 |
| LC::doiAction START | 0.000180 | 0.026781 |
| LC::doiAction END to showListing | 0.168625 | 0.195406 |
| LC::showListing START | 0.000008 | 0.195414 |
| LC::showListing get reviews START | 0.003153 | 0.198567 |
| ES Review Search START | 0.006651 | 0.205218 |
| ES Review Search END | 0.006239 | 0.211457 |
| LC::showListing get reviews END | 0.002068 | 0.213525 |
| Done | 0.031332 | 0.244857 |
Good synthesis but experimental lacking some useful details
The preparation of tetramethylguanidium azide was successfully carried out following the literature preparation (JOC 31, 1426 (1966)). Hydrazoic acid was prepared as a Et2O solution by adding conc HCl over 30 minutes to a ice cold solution of NaN3 in water followed by an...