| /paper/doi/10.1021/jo01343a026 | 0.000000 | 0.000000 |
| INIT | 0.000237 | 0.000237 |
| _initView | 0.000997 | 0.001234 |
| _initViewBasic | 0.000179 | 0.001413 |
| _initSiteModules | 0.000178 | 0.001591 |
| _initRouters | 0.000162 | 0.001753 |
| Sess + | 0.001559 | 0.003312 |
| Sess _ | 0.000103 | 0.003415 |
| pre dispatch _ | 0.000153 | 0.003568 |
| LC::doiAction START | 0.000236 | 0.003804 |
| LC::doiAction END to showListing | 0.161823 | 0.165627 |
| LC::showListing START | 0.000004 | 0.165631 |
| LC::showListing get reviews START | 0.000017 | 0.165648 |
| ES Review Search START | 0.000713 | 0.166361 |
| ES Review Search END | 0.008303 | 0.174664 |
| LC::showListing get reviews END | 0.000821 | 0.175485 |
| Done | 0.027090 | 0.202575 |
Good synthesis but experimental lacking some useful details
The preparation of tetramethylguanidium azide was successfully carried out following the literature preparation (JOC 31, 1426 (1966)). Hydrazoic acid was prepared as a Et2O solution by adding conc HCl over 30 minutes to a ice cold solution of NaN3 in water followed by an...