| /paper/doi/10.1021/jo01343a026 | 0.000000 | 0.000000 |
| INIT | 0.002907 | 0.002907 |
| _initView | 0.009056 | 0.011963 |
| _initViewBasic | 0.000879 | 0.012842 |
| _initSiteModules | 0.001412 | 0.014254 |
| _initRouters | 0.001529 | 0.015783 |
| pre dispatch _ | 0.013134 | 0.028917 |
| LC::doiAction START | 0.000190 | 0.029107 |
| LC::doiAction END to showListing | 0.174217 | 0.203324 |
| LC::showListing START | 0.000005 | 0.203329 |
| LC::showListing get reviews START | 0.003446 | 0.206775 |
| ES Review Search START | 0.006524 | 0.213299 |
| ES Review Search END | 0.007495 | 0.220794 |
| LC::showListing get reviews END | 0.002413 | 0.223207 |
| Done | 0.040047 | 0.263254 |
Good synthesis but experimental lacking some useful details
The preparation of tetramethylguanidium azide was successfully carried out following the literature preparation (JOC 31, 1426 (1966)). Hydrazoic acid was prepared as a Et2O solution by adding conc HCl over 30 minutes to a ice cold solution of NaN3 in water followed by an...