| /paper/doi/10.1021/jo01343a026 | 0.000000 | 0.000000 |
| INIT | 0.008653 | 0.008653 |
| _initView | 0.020740 | 0.029393 |
| _initViewBasic | 0.003681 | 0.033074 |
| _initSiteModules | 0.001734 | 0.034808 |
| _initRouters | 0.001690 | 0.036498 |
| pre dispatch _ | 0.029420 | 0.065918 |
| LC::doiAction START | 0.000185 | 0.066103 |
| LC::doiAction END to showListing | 0.237679 | 0.303782 |
| LC::showListing START | 0.000007 | 0.303789 |
| LC::showListing get reviews START | 0.009692 | 0.313481 |
| ES Review Search START | 0.010504 | 0.323985 |
| ES Review Search END | 0.005809 | 0.329794 |
| LC::showListing get reviews END | 0.002128 | 0.331922 |
| Done | 0.069176 | 0.401098 |
Good synthesis but experimental lacking some useful details
The preparation of tetramethylguanidium azide was successfully carried out following the literature preparation (JOC 31, 1426 (1966)). Hydrazoic acid was prepared as a Et2O solution by adding conc HCl over 30 minutes to a ice cold solution of NaN3 in water followed by an...