| /paper/doi/10.1021/jo01343a026 | 0.000000 | 0.000000 |
| INIT | 0.003563 | 0.003563 |
| _initView | 0.010974 | 0.014537 |
| _initViewBasic | 0.001079 | 0.015616 |
| _initSiteModules | 0.001803 | 0.017419 |
| _initRouters | 0.001913 | 0.019332 |
| pre dispatch _ | 0.016996 | 0.036328 |
| LC::doiAction START | 0.000231 | 0.036559 |
| LC::doiAction END to showListing | 0.203195 | 0.239754 |
| LC::showListing START | 0.000013 | 0.239767 |
| LC::showListing get reviews START | 0.011077 | 0.250844 |
| ES Review Search START | 0.011739 | 0.262583 |
| ES Review Search END | 0.010134 | 0.272717 |
| LC::showListing get reviews END | 0.004192 | 0.276909 |
| Done | 0.050877 | 0.327786 |
Good synthesis but experimental lacking some useful details
The preparation of tetramethylguanidium azide was successfully carried out following the literature preparation (JOC 31, 1426 (1966)). Hydrazoic acid was prepared as a Et2O solution by adding conc HCl over 30 minutes to a ice cold solution of NaN3 in water followed by an...