Synthesis and Azidolysis of 2-Chlorotetramethylguanidine. Synthetic Utility of Hexa- and Tetramethylguanidinium Azide

Anthony J. Papa

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DOI 10.1021/jo01343a026

Journal The Journal of Organic Chemistry
Location p 1426-1430, Volume 31, Issue 5, 1966
Publication Type journal-article

Tags organic chemistry
Publisher Link Click Here

Review

14 Jan 2017

Bobbie Dorow

(6)

Good synthesis but experimental lacking some useful details

The preparation of tetramethylguanidium azide was successfully carried out following the literature preparation (JOC 31, 1426 (1966)). Hydrazoic acid was prepared as a Et2O solution by adding conc HCl over 30 minutes to a ice cold solution of NaN3 in water followed by an...

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Synthesis and Azidolysis of 2-Chlorotetramethylguanidine. Synthetic Utility of Hexa- and Tetramethylguanidinium Azide

Anthony J. Papa

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Good synthesis but experimental lacking some useful details

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