Synthesis and Azidolysis of 2-Chlorotetramethylguanidine. Synthetic Utility of Hexa- and Tetramethylguanidinium Azide

Anthony J. Papa

Add Review (press R) Confirm Authorship

Paper Rating

Paper Details

DOI 10.1021/jo01343a026

Journal The Journal of Organic Chemistry
Location p 1426-1430, Volume 31, Issue 5, 1966
Publication Type journal-article

Tags organic chemistry
Publisher Link Click Here

Review

14 Jan 2017

Bobbie Dorow

(6)

Good synthesis but experimental lacking some useful details

The preparation of tetramethylguanidium azide was successfully carried out following the literature preparation (JOC 31, 1426 (1966)). Hydrazoic acid was prepared as a Et2O solution by adding conc HCl over 30 minutes to a ice cold solution of NaN3 in water followed by an...

/paper/doi/10.1021/jo01343a026	0.000000	0.000000
INIT	0.000212	0.000212
_initView	0.000906	0.001118
_initViewBasic	0.000195	0.001313
_initSiteModules	0.000164	0.001477
_initRouters	0.000150	0.001627
Sess +	0.001466	0.003093
Sess _	0.000098	0.003191
pre dispatch _	0.000134	0.003325
LC::doiAction START	0.000210	0.003535
LC::doiAction END to showListing	0.152390	0.155925
LC::showListing START	0.000005	0.155930
LC::showListing get reviews START	0.000017	0.155947
ES Review Search START	0.000647	0.156594
ES Review Search END	0.005019	0.161613
LC::showListing get reviews END	0.000813	0.162426
Done	0.026294	0.188720

Loading...

Synthesis and Azidolysis of 2-Chlorotetramethylguanidine. Synthetic Utility of Hexa- and Tetramethylguanidinium Azide

Anthony J. Papa

Overall Rating

Review

Good synthesis but experimental lacking some useful details

Recently Reviewed

Has Cited

Cited by

Sign In With