| /paper/doi/10.1021/jo01343a026 | 0.000000 | 0.000000 |
| INIT | 0.005445 | 0.005445 |
| _initView | 0.009589 | 0.015034 |
| _initViewBasic | 0.001122 | 0.016156 |
| _initSiteModules | 0.001638 | 0.017794 |
| _initRouters | 0.001683 | 0.019477 |
| pre dispatch _ | 0.015020 | 0.034497 |
| LC::doiAction START | 0.000213 | 0.034710 |
| LC::doiAction END to showListing | 0.178429 | 0.213139 |
| LC::showListing START | 0.000004 | 0.213143 |
| LC::showListing get reviews START | 0.000016 | 0.213159 |
| ES Review Search START | 0.006471 | 0.219630 |
| ES Review Search END | 0.009736 | 0.229366 |
| LC::showListing get reviews END | 0.002263 | 0.231629 |
| Done | 0.035877 | 0.267506 |
Good synthesis but experimental lacking some useful details
The preparation of tetramethylguanidium azide was successfully carried out following the literature preparation (JOC 31, 1426 (1966)). Hydrazoic acid was prepared as a Et2O solution by adding conc HCl over 30 minutes to a ice cold solution of NaN3 in water followed by an...