Structural and conformational studies of 2-phenyl-1,3,2-diaza- and -dioxaboracycloalkanes

  • 10.1021/jo00975a027
  • The Journal of Organic Chemistry
  • p 1583-1587, Volume 37, Issue 10,
  • journal-article


Experimental Details

t-Bu amine (50 mmol) and methyl acrylate (50 mmol) were dissolved in MeOH (10 mL) and stirred overnight under nitrogen.  The secondary amine was isolated by Kugelrohr distillation after the MeOH had been removed by rotary evaporation.  The purified material was dissolved in Et2O...