Structural and conformational studies of 2-phenyl-1,3,2-diaza- and -dioxaboracycloalkanes

Ignatius J. Turchi , Bruce E. Maryanoff , Robert O. Hutchins , Franklin A. Davis

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DOI 10.1021/jo00975a027

Journal The Journal of Organic Chemistry
Location p 1583-1587, Volume 37, Issue 10, 1972
Publication Type journal-article

Tags organic chemistry
Publisher Link Click Here

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19 Dec 2016

Bobbie Dorow

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Experimental Details

t-Bu amine (50 mmol) and methyl acrylate (50 mmol) were dissolved in MeOH (10 mL) and stirred overnight under nitrogen. The secondary amine was isolated by Kugelrohr distillation after the MeOH had been removed by rotary evaporation. The purified material was dissolved in Et2O...

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Structural and conformational studies of 2-phenyl-1,3,2-diaza- and -dioxaboracycloalkanes

Ignatius J. Turchi , Bruce E. Maryanoff , Robert O. Hutchins , Franklin A. Davis

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