One-Step Synthesis of TiO2(B) Nanoparticles from a Water-Soluble Titanium Complex

  • 10.1021/cm071370q
  • Chem. Mater.
  • p 5-3, 19 (22),
For the first time, TiO 2 (B) was obtained by a one-step procedure. The hydrothermal synthesis is carried out under acidic conditions in 0.59 M H 2 SO 4 solution at 160−200 °C using titanium complex with glycolic acid. The obtained nanoparticles were characterized by XRD, Raman spectroscopy, and TEM.